2025 Journal of esthetic and resto…

Role of Amine and/or Tin-Containing Dentifrices on Tooth Discoloration and Surface Properties.

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Journal of esthetic and restorative dentistry : official publication of the American Academy of Esthetic Dentistry ... [et al.] Vol. 37 (6) : 1585-1592 • Jun 2025

OBJECTIVE: This study evaluated the impact of dentifrices containing amine fluoride (AmF) and/or tin on tooth discoloration and surface roughness under cycles of staining and abrasion. MATERIALS AND METHODS: Specimens of enamel (n = 10) and dentin (n = 19) were allocated into six groups: (1) Negative control (Distilled water), (2) NaF (regular fluoridated dentifrice without amine and tin), (3) AmF, (4) AmF/NaF/SnCl(2), (5) SnF(2)/SnCl(2), and (6) SnF(2). Daily staining-toothbrushing cycling was performed: staining solution (30 min), toothbrushing (45 strokes), and human saliva (1 h), 2x/day, for 21 days. Tooth color change (DeltaE, DeltaL, Deltaa, and Deltab) was determined using a spectrophotometer (CIEDE2000), while surface roughness (DeltaRa) was measured with an optical profilometer, and the data were statistically analyzed (alpha = 0.05). RESULTS: For enamel, no significant differences in DeltaE were observed among groups; however, for dentin, AmF exhibited the highest DeltaE value, differing from all groups except Negative control (p > 0.05). Both substrates showed a decrease in luminosity (-DeltaL), with significant differences in dentin for the AmF group (p < 0.05). For dentin, all groups showed an increase in tooth yellowness (+Deltab); while for enamel, only the tin-containing groups showed this effect. All groups showed an increase in surface roughness after cycling. Enamel Ra showed significant differences post-treatment, with AmF differing from NaF/AmF/SnCl(2) (p = 0.012) and control (p = 0.042). Correlations between DeltaRa and DeltaE were weak in both substrates (rho = 0.12 for enamel; rho = 0.22 for dentin). CONCLUSIONS: Brushing with AmF/NaF/SnCl(2), SnF(2)/SnCl(2), and SnF(2)-containing toothpastes promoted a yellowing of enamel. Brushing with AmF resulted in the greatest darkening of dentin compared with other fluoride salts. CLINICAL SIGNIFICANCE: Some components in dentifrices can induce tooth discoloration, which seems to impact dental aesthetics; therefore, clinicians should advise patients on potential color alterations when choosing specific dentifrice products.

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